基于GC-MS的陈皮不同炮制品挥发性成分定性研究
投稿时间:2019-09-17     点此下载全文
引用本文:潘盼盼,孙戡平,郑艳萍,金俊杰,李淑佩.基于GC-MS的陈皮不同炮制品挥发性成分定性研究[J].中国现代中药,2020,22(9):1463-1469
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作者中文名作者英文名单位中文名单位英文名E-Mail
潘盼盼 PAN Pan-pan 南京医科大学附属妇产科医院(南京市妇幼保健院),江苏南京210004 Nanjing Maternity and Child Health Hospital,Nanjing 210004,China  
孙戡平 SUN Kan-ping 南京海昌中药集团有限公司,江苏南京210061 Nanjing Haichang Chinese Medicine Group Co.,Ltd.,Nanjing 210061,China  
郑艳萍 ZHENG Yan-ping 南京海昌中药集团有限公司,江苏南京210061 Nanjing Haichang Chinese Medicine Group Co.,Ltd.,Nanjing 210061,China  
金俊杰 JIN Jun-jie 南京海昌中药集团有限公司,江苏南京210061 Nanjing Haichang Chinese Medicine Group Co.,Ltd.,Nanjing 210061,China  
李淑佩 LI Shu-pei 江苏省中医院,江苏南京210029 Jiangsu Provincial Hospital of Traditional Chinese Medicine,Nanjing 210029,China 李淑佩,主管药师,研究方向:药房配方;E-mail:3595344275@qq.com 
基金项目:国家中医药管理局公益性行业专项(201507002-2)
中文摘要:目的:研究陈皮醋制、麸炒、蜜制、土炒4种炮制品挥发油成分的种类及其差异。方法:利用气相色谱-质谱(GC-MS)法,HP-5MS色谱柱;载气为高纯度氦气;进样量1 μL;分流比300∶1;程序升温,检测陈皮4种炮制品挥发油成分。结果:在陈皮4种炮制品中测定到的挥发性成分共180种,其中含量最高的均为柑橘柠烯(D-limoneoe),是1种单萜类化合物;醋制陈皮和土炒陈皮所含柑橘柠烯质量分数最高,分别为76.86%和72.56%。结论:该方法稳定可靠,初步探讨了陈皮4种不同炮制品中挥发油种类及含量。
中文关键词:陈皮  醋制  麸炒  蜜制  土炒  挥发油
 
Qualitative Study on Volatile Components of Different Citri Reticulatae Pericarpium Products Based on GC-MS
Abstract:Objective:To study the differences of volatile oil components in four processed products of Citri Reticulatae Pericarpium,including vinegar,bran,honey and soil preparation. Methods:GC-MS chromatography with HP-5MS chromatography column was applied in the study. The carrier gas was high purity helium,the injection volume was 1 μL,and the ratio of diversion was 300∶1. The volatile oil components of four processed products of Citri Reticulatae Pericarpium were detected under programmed heating conditions. Results:A total of 180 volatile components were detected in the above four processed products of Citri Reticulatae Pericarpium,of which D-limonene was the highest,which was a monoterpene compound. The citrus limonene content in vinegar-processed Citri Reticulatae Pericarpium and parched Citri Reticulatae Pericarpium was the highest,76.86% and 72.56%,respectively. Conclusion:The method is stable and reliable. The types and contents of volatile oil in four different processed products of Citri Reticulatae Pericarpium were preliminarily discussed.
keywords:Citri Reticulatae Pericarpium  processing with vinegar  bran frying  honey preparation  soil preparation  volatile oil
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